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A non-destructive sampling method for food authentication using gas chromatography coupled to mass spectrometry or ion mobility spectrometry

Autores

SEGURA BORREGO, MARIA PILAR, Martin-Gomez, A. , Rios-Reina, R. , Cardador, M. J. , Morales, M. L. , Arce, L. , Callejon, R. M.

Publicación externa

No

Medio

Food Chem

Alcance

Article

Naturaleza

Científica

Cuartil JCR

1

Cuartil SJR

1

Impacto JCR

8.8

Impacto SJR

1.624

Fecha de publicacion

30/03/2022

ISI

000734135900012

Abstract

The study of volatile compounds obtained by gas chromatography (GC) coupled to mass spectrometry (MS) or ion mobility spectrometry (IMS) may be very useful to protect food quality, especially when using a nondestructive sampling method. In this work, the authentication of the highly appreciated dry-cured Iberian ham by those techniques was studied and compared. The results obtained show the suitability of a nondestructive sampling method coupled to headspace sampling (HS)-GC-IMS or HS-GC-MS to determine volatile markers in the feeding Iberian pig regime. Although both methods were suitable to differentiate the ham categories, HS-GC-IMS was more sensitive detecting a higher number of compounds than HS-GC-MS, which provided accurate qualitative results. The results of principal component analysis showed that ethanol, 2-propanol and 3methylbutanol, identified by HS-GC-IMS, and 3-methylbutanal and heptane, identified by HS-GC-MS, could be considered potential markers to identify ham from different feeding regimes.

Palabras clave

Dry-cured Iberia n ham; HS-GC -MS; HS-GC-IMS; Acorn-fed; Feed-f e d; Non-destructive sampling

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